Abstract
A simple, efficient ad economical synthesis technique for the fabrication of core shell structures was reported, where the metallic mercury forms the core. The meta/carbon core shell structures of an Hg/C compound is prepared by the thermolysis of an Hg(CH3)2. X-ray powder diffraction data were obtained by means of a horizontally mounted, INEL cylindrical position-sensitive detector. External calibration using the Na 2Ca3AI2F4 cubic phase was applied by means of cubic spline fittings. The peak positions were determined by pseudo-Voight fittings. The liquid samples were sealed in 0.3 mm diameter Lindemann capillaries. which rotated perpendicularly to the X-ray beam during the experiments. It was observed that the Hg/C particles exhibited interesting surface features that can be exploited in catalysis. The adopted method is generally applicable for all alkyl-metal compounds.
Original language | English |
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Pages (from-to) | 1000-1002 |
Number of pages | 3 |
Journal | Advanced Materials |
Volume | 20 |
Issue number | 5 |
DOIs | |
State | Published - 5 Mar 2008 |