Synthesis, structural and morphological analysis of hexagonal boron nitride doped BaCO3-TiO2composites

Abhishek Madheshiya; Sarvesh Kumar Avinashi; Swajal Kumar Srivastava; Subodh Kumar; Chandkiram Gautam

doi:10.1016/j.matpr.2020.05.282

Synthesis, structural and morphological analysis of hexagonal boron nitride doped BaCO₃-TiO₂composites

Abhishek Madheshiya, Sarvesh Kumar Avinashi, Swajal Kumar Srivastava, Subodh Kumar, Chandkiram Gautam

Research output: Contribution to journal › Conference article › peer-review

4 Scopus citations

Abstract

Various compositions of hexagonal boron nitride (h-BN) doped ceramics in the compound [(70-x)BaCO3-30TiO2-xBN] (xâ€»=â€»0, 1, 3, and 5) were prepared using conventional solid-state reaction method. X-ray diffraction (XRD) analysis showed the formation of bulk and opaque samples that confirmed the highly crystalline nature of these ceramics. The structural, surface morphological and elemental analyses were carried out in brief by employing the distinct characterization techniques. To obtain the information about the bond formation among the used oxides/nitride in these composite ceramics the FTIR tests were performed. Scanning electron microscope (SEM) was used to record the surface features at a desired magnification of the ceramic samples along with their grain and grain boundary distributions. The energy dispersive X-ray analysis (EDAX) was also carried out in detail for the Gold (Au) coated ceramic samples and determines the average elemental compositions.

Original language	English
Pages (from-to)	457-463
Number of pages	7
Journal	Materials Today: Proceedings
Volume	31
DOIs	https://doi.org/10.1016/j.matpr.2020.05.282
State	Published - 2019
Externally published	Yes
Event	14th International Conference on Advanced Nano Materials, ANM 2019 - Aviero, Portugal Duration: 17 Jul 2019 → 19 Jul 2019

Bibliographical note

Publisher Copyright:
© 2019 Elsevier Ltd.

Funding

C. R. Gautam admiringly acknowledged the Science and Engineering Research Board, Department of Science and Technology (SERB-DST) New Delhi, India for providing the monetary support under Empowerment and Equity Opportunities for Excellence in Science (File No. EEO/2018/000647) as a major research project. Authors are also conveying a sincere thanks to the Centre of ESUP Scheme Government for extending the powder XRD facility at the Department of Physics, University of Lucknow. A. Madheshiya is thankfully recognized to the Council of Scientific and Industrial Research-Human Resource Development Group , CSIR Complex, Pusa, New Delhi (India) for providing the financial help under ‘Senior Research Fellowship’ no. 09/107(0380)/2016-EMR-I (Ack. No. 124250/2K15/1).

Funders	Funder number
Department of Science and Technology, Ministry of Science and Technology, India
Science and Engineering Research Board
Council of Scientific and Industrial Research, India	124250/2K15/1, 09/107(0380)/2016-EMR-I
SERB-DST	EEO/2018/000647
Council of Scientific and Industrial Research-Human Resource Development Group

Keywords

EDAX
FTIR spectroscopy
Surface morphology
Synthesis
XRD

Access to Document

10.1016/j.matpr.2020.05.282

Cite this

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title = "Synthesis, structural and morphological analysis of hexagonal boron nitride doped BaCO3-TiO2composites",

abstract = "Various compositions of hexagonal boron nitride (h-BN) doped ceramics in the compound [(70-x)BaCO3-30TiO2-xBN] (x{\^a}€»={\^a}€»0, 1, 3, and 5) were prepared using conventional solid-state reaction method. X-ray diffraction (XRD) analysis showed the formation of bulk and opaque samples that confirmed the highly crystalline nature of these ceramics. The structural, surface morphological and elemental analyses were carried out in brief by employing the distinct characterization techniques. To obtain the information about the bond formation among the used oxides/nitride in these composite ceramics the FTIR tests were performed. Scanning electron microscope (SEM) was used to record the surface features at a desired magnification of the ceramic samples along with their grain and grain boundary distributions. The energy dispersive X-ray analysis (EDAX) was also carried out in detail for the Gold (Au) coated ceramic samples and determines the average elemental compositions.",

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author = "Abhishek Madheshiya and {Kumar Avinashi}, Sarvesh and {Kumar Srivastava}, Swajal and Subodh Kumar and Chandkiram Gautam",

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AU - Madheshiya, Abhishek

AU - Kumar Avinashi, Sarvesh

AU - Kumar Srivastava, Swajal

AU - Kumar, Subodh

AU - Gautam, Chandkiram

PY - 2019

Y1 - 2019

N2 - Various compositions of hexagonal boron nitride (h-BN) doped ceramics in the compound [(70-x)BaCO3-30TiO2-xBN] (xâ€»=â€»0, 1, 3, and 5) were prepared using conventional solid-state reaction method. X-ray diffraction (XRD) analysis showed the formation of bulk and opaque samples that confirmed the highly crystalline nature of these ceramics. The structural, surface morphological and elemental analyses were carried out in brief by employing the distinct characterization techniques. To obtain the information about the bond formation among the used oxides/nitride in these composite ceramics the FTIR tests were performed. Scanning electron microscope (SEM) was used to record the surface features at a desired magnification of the ceramic samples along with their grain and grain boundary distributions. The energy dispersive X-ray analysis (EDAX) was also carried out in detail for the Gold (Au) coated ceramic samples and determines the average elemental compositions.

AB - Various compositions of hexagonal boron nitride (h-BN) doped ceramics in the compound [(70-x)BaCO3-30TiO2-xBN] (xâ€»=â€»0, 1, 3, and 5) were prepared using conventional solid-state reaction method. X-ray diffraction (XRD) analysis showed the formation of bulk and opaque samples that confirmed the highly crystalline nature of these ceramics. The structural, surface morphological and elemental analyses were carried out in brief by employing the distinct characterization techniques. To obtain the information about the bond formation among the used oxides/nitride in these composite ceramics the FTIR tests were performed. Scanning electron microscope (SEM) was used to record the surface features at a desired magnification of the ceramic samples along with their grain and grain boundary distributions. The energy dispersive X-ray analysis (EDAX) was also carried out in detail for the Gold (Au) coated ceramic samples and determines the average elemental compositions.

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