Abstract
Ammonium trichloro (dioxyethylene-O,O') tellurate(IV) (AS-101) was sythesized by refluxing tellurium(IV) chloride and ethylene glycol in acetonitrile, or by refluxing tellurium(IV) chloride and ammonium chloride in ethylene glycol. A mechanism for the reaction is suggested. X-ray data for AS-101 are given. Replacing ammonium chloride by potassium chloride yielded the potassium salt; however, with sodium chloride the sodium salt was not obtained.
Original language | English |
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Pages (from-to) | 635-636 |
Number of pages | 2 |
Journal | Synthesis (Germany) |
Volume | 1989 |
Issue number | 8 |
DOIs | |
State | Published - 1989 |
Bibliographical note
Publisher Copyright:© 1989 Georg Thieme Verlag. All rights reserved.