Stannous chloride reduction of nitroalkenes in amines. Synthesis and cycloaddition of α-dialkylaminoaldoxime

Levi Gottlieb; Alfred Hassner; Hugo E. Gottlieb

doi:10.1080/00397910008087409

Stannous chloride reduction of nitroalkenes in amines. Synthesis and cycloaddition of α-dialkylaminoaldoxime

Levi Gottlieb, Alfred Hassner, Hugo E. Gottlieb

Department of Chemistry

Ministry of Defence, Government of Israel

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

α-Dialkylamino aldoximes 12 were prepared by stannous chloride reduction of nitroalkenes in amines. An intramolecular Michael addition- deoxygenation mechanism is suggested. α-Allylamino aldoxime underwent an efficient Intramolecular Oxime Olefin Cycloaddition (IOOC) giving 13.

Original language	English
Pages (from-to)	2445-2464
Number of pages	20
Journal	Synthetic Communications
Volume	30
Issue number	14
DOIs	https://doi.org/10.1080/00397910008087409
State	Published - 2000

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Funding Information:
Acknowledgment: Support for this research by a grant from the Israel Research

Funding

Acknowledgment: Support for this research by a grant from the Israel Research

Funders	Funder number
Israel Research

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10.1080/00397910008087409

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abstract = "α-Dialkylamino aldoximes 12 were prepared by stannous chloride reduction of nitroalkenes in amines. An intramolecular Michael addition- deoxygenation mechanism is suggested. α-Allylamino aldoxime underwent an efficient Intramolecular Oxime Olefin Cycloaddition (IOOC) giving 13.",

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AU - Hassner, Alfred

AU - Gottlieb, Hugo E.

N1 - Funding Information: Acknowledgment: Support for this research by a grant from the Israel Research

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AB - α-Dialkylamino aldoximes 12 were prepared by stannous chloride reduction of nitroalkenes in amines. An intramolecular Michael addition- deoxygenation mechanism is suggested. α-Allylamino aldoxime underwent an efficient Intramolecular Oxime Olefin Cycloaddition (IOOC) giving 13.

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Stannous chloride reduction of nitroalkenes in amines. Synthesis and cycloaddition of α-dialkylaminoaldoxime

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