Preparation de l'acide méso diamino‐2, 6 heptane‐dioique‐1, 7‐[3H‐3, 4, 5] (méso‐diamino pimelique‐[3H‐3, 4, 5])

D. Schott; B. Rousseau; J. P. Beaucourt; J. P. Lellouche; L. Pichat

doi:10.1002/jlcr.2580220205

Preparation de l'acide méso diamino‐2, 6 heptane‐dioique‐1, 7‐[³H‐3, 4, 5] (méso‐diamino pimelique‐[³H‐3, 4, 5])

D. Schott, B. Rousseau, J. P. Beaucourt, J. P. Lellouche, L. Pichat

Serv. des Molecules Marquees

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

Meso 2, 6‐diamino [³H‐3, 4, 5] 1, 7‐heptanedioc acid‐ (meso [³H‐3, 4, 5] DAP) specific activity 30 Ci/mM was obtained by catalytic dehydrohalogenation of meso 3‐chloro and 4‐chloro DAP. LL, DD and meso DAP were analytically separated by cellulose thin layer chromatography (methanol‐water‐7 : 3).

Original language	French
Pages (from-to)	127-133
Number of pages	7
Journal	Journal of Labelled Compounds and Radiopharmaceuticals
Volume	22
Issue number	2
DOIs	https://doi.org/10.1002/jlcr.2580220205
State	Published - Feb 1985
Externally published	Yes

Keywords

Catalytic dehydrohalogenation
Cellulose thin layer chromatography
Meso 4‐chloro DAP
Meso 5‐chloro DAP
meso 2, 6‐diamino 1, 7‐heptanedioic acid‐[H‐3, 4, 5]

Access to Document

10.1002/jlcr.2580220205

Cite this

@article{f75f6c8008854b258a34c3b52c072e04,

title = "Preparation de l'acide m{\'e}so diamino‐2, 6 heptane‐dioique‐1, 7‐[3H‐3, 4, 5] (m{\'e}so‐diamino pimelique‐[3H‐3, 4, 5])",

abstract = "Meso 2, 6‐diamino [3H‐3, 4, 5] 1, 7‐heptanedioc acid‐ (meso [3H‐3, 4, 5] DAP) specific activity 30 Ci/mM was obtained by catalytic dehydrohalogenation of meso 3‐chloro and 4‐chloro DAP. LL, DD and meso DAP were analytically separated by cellulose thin layer chromatography (methanol‐water‐7 : 3).",

keywords = "Catalytic dehydrohalogenation, Cellulose thin layer chromatography, Meso 4‐chloro DAP, Meso 5‐chloro DAP, meso 2, 6‐diamino 1, 7‐heptanedioic acid‐[H‐3, 4, 5]",

author = "D. Schott and B. Rousseau and Beaucourt, {J. P.} and Lellouche, {J. P.} and L. Pichat",

year = "1985",

month = feb,

doi = "10.1002/jlcr.2580220205",

language = "צרפתית",

volume = "22",

pages = "127--133",

journal = "Journal of Labelled Compounds and Radiopharmaceuticals",

issn = "0362-4803",

publisher = "John Wiley and Sons Ltd",

number = "2",

}

TY - JOUR

T1 - Preparation de l'acide méso diamino‐2, 6 heptane‐dioique‐1, 7‐[3H‐3, 4, 5] (méso‐diamino pimelique‐[3H‐3, 4, 5])

AU - Schott, D.

AU - Rousseau, B.

AU - Beaucourt, J. P.

AU - Lellouche, J. P.

AU - Pichat, L.

PY - 1985/2

Y1 - 1985/2

N2 - Meso 2, 6‐diamino [3H‐3, 4, 5] 1, 7‐heptanedioc acid‐ (meso [3H‐3, 4, 5] DAP) specific activity 30 Ci/mM was obtained by catalytic dehydrohalogenation of meso 3‐chloro and 4‐chloro DAP. LL, DD and meso DAP were analytically separated by cellulose thin layer chromatography (methanol‐water‐7 : 3).

AB - Meso 2, 6‐diamino [3H‐3, 4, 5] 1, 7‐heptanedioc acid‐ (meso [3H‐3, 4, 5] DAP) specific activity 30 Ci/mM was obtained by catalytic dehydrohalogenation of meso 3‐chloro and 4‐chloro DAP. LL, DD and meso DAP were analytically separated by cellulose thin layer chromatography (methanol‐water‐7 : 3).

KW - Catalytic dehydrohalogenation

KW - Cellulose thin layer chromatography

KW - Meso 4‐chloro DAP

KW - Meso 5‐chloro DAP

KW - meso 2, 6‐diamino 1, 7‐heptanedioic acid‐[H‐3, 4, 5]

UR - http://www.scopus.com/inward/record.url?scp=0021923415&partnerID=8YFLogxK

U2 - 10.1002/jlcr.2580220205

DO - 10.1002/jlcr.2580220205

M3 - ???researchoutput.researchoutputtypes.contributiontojournal.article???

AN - SCOPUS:0021923415

SN - 0362-4803

VL - 22

SP - 127

EP - 133

JO - Journal of Labelled Compounds and Radiopharmaceuticals

JF - Journal of Labelled Compounds and Radiopharmaceuticals

IS - 2