Skip to main navigation Skip to search Skip to main content

NMR chemical shifts of trace impurities: Common laboratory solvents, organics, and gases in deuterated solvents relevant to the organometallic chemist

  • Gregory R. Fulmer
  • , Alexander J.M. Miller
  • , Nathaniel H. Sherden
  • , Hugo E. Gottlieb
  • , Abraham Nudelman
  • , Brian M. Stoltz
  • , John E. Bercaw
  • , Karen I. Goldberg
  • University of Washington
  • California Institute of Technology

Research output: Contribution to journalArticlepeer-review

3584 Scopus citations

Abstract

Tables of 1H and 13C NMR chemical shifts have been compiled for common organic compounds often used as reagents or found as products or contaminants in deuterated organic solvents. Building upon the work of Gottlieb, Kotlyar, and Nudelman in the Journal of Organic Chemistry, signals for common impurities are now reported in additional NMR solvents (tetrahydrofuran-d8, toluene-d8, dichloromethane-d 2, chlorobenzene-d5, and 2,2,2-trifluoroethanol-d 3) which are frequently used in organometallic laboratories. Chemical shifts for other organics which are often used as reagents or internal standards or are found as products in organometallic chemistry are also reported for all the listed solvents.

Original languageEnglish
Pages (from-to)2176-2179
Number of pages4
JournalOrganometallics
Volume29
Issue number9
DOIs
StatePublished - 10 May 2010

Fingerprint

Dive into the research topics of 'NMR chemical shifts of trace impurities: Common laboratory solvents, organics, and gases in deuterated solvents relevant to the organometallic chemist'. Together they form a unique fingerprint.

Cite this