TY - JOUR
T1 - Microwave assisted preparation of binary oxide nanoparticles
AU - Palchik, Oleg
AU - Zhu, Junjie
AU - Gedanken, Aharon
PY - 2000
Y1 - 2000
N2 - A group of binary oxide nanophase materials were prepared using a microwave assisted soft-chemical route. BaTiO3, Ba6Ti17O40, BaZrO3 and PbTiO3 were prepared from BaCl2 hydrate, Pb(Ac)2, Ti(OPr(i))4 and ZrOCl2. All reactions were performed in ethylene glycol, which acted as both a solvent and a growth regulating agent, under atmospheric pressure in a microwave reactor. The products that were obtained were analyzed by using XRD, TEM, XPS, EDX and FT-IR.
AB - A group of binary oxide nanophase materials were prepared using a microwave assisted soft-chemical route. BaTiO3, Ba6Ti17O40, BaZrO3 and PbTiO3 were prepared from BaCl2 hydrate, Pb(Ac)2, Ti(OPr(i))4 and ZrOCl2. All reactions were performed in ethylene glycol, which acted as both a solvent and a growth regulating agent, under atmospheric pressure in a microwave reactor. The products that were obtained were analyzed by using XRD, TEM, XPS, EDX and FT-IR.
UR - http://www.scopus.com/inward/record.url?scp=0034111009&partnerID=8YFLogxK
U2 - 10.1039/a908795h
DO - 10.1039/a908795h
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AN - SCOPUS:0034111009
SN - 0959-9428
VL - 10
SP - 1251
EP - 1254
JO - Journal of Materials Chemistry
JF - Journal of Materials Chemistry
IS - 5
ER -