Microwave-Assisted Polyol Synthesis of CulnTe2 and CulnSe 2 Nanoparticles

Haviv Grisaru; Oleg Palchik; Aharon Gedanken; Valery Palchik; Michael A. Slifkin; Arie M. Weiss

doi:10.1021/ic0342853

Microwave-Assisted Polyol Synthesis of CulnTe₂ and CulnSe ₂ Nanoparticles

Haviv Grisaru, Oleg Palchik, Aharon Gedanken, Valery Palchik, Michael A. Slifkin, Arie M. Weiss

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

139 Scopus citations

Abstract

Nanoparticles of the CulnTe₂ (CIT) and CulnSe₂ (CIS) alloys have been prepared using the microwave-assisted polyol method. In this simple and quick reaction the polyol is both the solvent and the reducing agent. XRD studies show that nanoparticles of CIT and CIS are formed in the body-centered tetragonal structure and their average diameters are ∼94 and ∼83 nm, respectively. Electron microscopy studies show that these formed particles are poorly aggregated with a mean diameter of 100 and 85 nm, respectively. The products have been characterized by different analytical techniques, and the electronic properties have been measured using photoacoustic spectroscopy (PAS).

Original language	English
Pages (from-to)	7148-7155
Number of pages	8
Journal	Inorganic Chemistry
Volume	42
Issue number	22
DOIs	https://doi.org/10.1021/ic0342853
State	Published - 3 Nov 2003

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abstract = "Nanoparticles of the CulnTe2 (CIT) and CulnSe2 (CIS) alloys have been prepared using the microwave-assisted polyol method. In this simple and quick reaction the polyol is both the solvent and the reducing agent. XRD studies show that nanoparticles of CIT and CIS are formed in the body-centered tetragonal structure and their average diameters are ∼94 and ∼83 nm, respectively. Electron microscopy studies show that these formed particles are poorly aggregated with a mean diameter of 100 and 85 nm, respectively. The products have been characterized by different analytical techniques, and the electronic properties have been measured using photoacoustic spectroscopy (PAS).",

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AU - Grisaru, Haviv

AU - Palchik, Oleg

AU - Gedanken, Aharon

AU - Palchik, Valery

AU - Slifkin, Michael A.

AU - Weiss, Arie M.

PY - 2003/11/3

Y1 - 2003/11/3

N2 - Nanoparticles of the CulnTe2 (CIT) and CulnSe2 (CIS) alloys have been prepared using the microwave-assisted polyol method. In this simple and quick reaction the polyol is both the solvent and the reducing agent. XRD studies show that nanoparticles of CIT and CIS are formed in the body-centered tetragonal structure and their average diameters are ∼94 and ∼83 nm, respectively. Electron microscopy studies show that these formed particles are poorly aggregated with a mean diameter of 100 and 85 nm, respectively. The products have been characterized by different analytical techniques, and the electronic properties have been measured using photoacoustic spectroscopy (PAS).

AB - Nanoparticles of the CulnTe2 (CIT) and CulnSe2 (CIS) alloys have been prepared using the microwave-assisted polyol method. In this simple and quick reaction the polyol is both the solvent and the reducing agent. XRD studies show that nanoparticles of CIT and CIS are formed in the body-centered tetragonal structure and their average diameters are ∼94 and ∼83 nm, respectively. Electron microscopy studies show that these formed particles are poorly aggregated with a mean diameter of 100 and 85 nm, respectively. The products have been characterized by different analytical techniques, and the electronic properties have been measured using photoacoustic spectroscopy (PAS).

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Microwave-Assisted Polyol Synthesis of CulnTe₂ and CulnSe ₂ Nanoparticles

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