Development of GSK's NMR guides-a tool to encourage the use of more sustainable solvents

Hugo E. Gottlieb; Grazyna Graczyk-Millbrandt; Graham G.A. Inglis; Abraham Nudelman; David Perez; Yanqiu Qian; Leanna E. Shuster; Helen F. Sneddon; Richard J. Upton

doi:10.1039/c6gc00446f

Development of GSK's NMR guides-a tool to encourage the use of more sustainable solvents

Hugo E. Gottlieb, Grazyna Graczyk-Millbrandt, Graham G.A. Inglis, Abraham Nudelman, David Perez, Yanqiu Qian, Leanna E. Shuster, Helen F. Sneddon, Richard J. Upton

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

23 Scopus citations

Abstract

Residual solvents often appear as nuisance signals in experimental NMR spectra, and many chemists turn to well-known literature sources to quickly identify such peaks. While these publications are very useful, they do not currently include many solvents exemplified in green chemistry-related literature. This work provides a single compiled reference for NMR chemical shifts of 80 solvents in each of 6 deuterated NMR solvents. The overall green chemistry assessments, as reached via the methodology of the GSK Solvent Sustainability Guide, are displayed on these charts.

Original language	English
Pages (from-to)	3867-3878
Number of pages	12
Journal	Green Chemistry
Volume	18
Issue number	13
DOIs	https://doi.org/10.1039/c6gc00446f
State	Published - 2016

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©2016 The Royal Society of Chemistry.

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title = "Development of GSK's NMR guides-a tool to encourage the use of more sustainable solvents",

abstract = "Residual solvents often appear as nuisance signals in experimental NMR spectra, and many chemists turn to well-known literature sources to quickly identify such peaks. While these publications are very useful, they do not currently include many solvents exemplified in green chemistry-related literature. This work provides a single compiled reference for NMR chemical shifts of 80 solvents in each of 6 deuterated NMR solvents. The overall green chemistry assessments, as reached via the methodology of the GSK Solvent Sustainability Guide, are displayed on these charts.",

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AU - Inglis, Graham G.A.

AU - Nudelman, Abraham

AU - Perez, David

AU - Qian, Yanqiu

AU - Shuster, Leanna E.

AU - Sneddon, Helen F.

AU - Upton, Richard J.

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AB - Residual solvents often appear as nuisance signals in experimental NMR spectra, and many chemists turn to well-known literature sources to quickly identify such peaks. While these publications are very useful, they do not currently include many solvents exemplified in green chemistry-related literature. This work provides a single compiled reference for NMR chemical shifts of 80 solvents in each of 6 deuterated NMR solvents. The overall green chemistry assessments, as reached via the methodology of the GSK Solvent Sustainability Guide, are displayed on these charts.

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Development of GSK's NMR guides-a tool to encourage the use of more sustainable solvents

Abstract

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