A novel sonochemical method for the preparation of nanophasic sulfides: Synthesis of HgS and PbS nanoparticles

Junjie Zhu; Suwen Liu; O. Palchik; Yuri Koltypin; A. Gedanken

doi:10.1006/jssc.2000.8780

A novel sonochemical method for the preparation of nanophasic sulfides: Synthesis of HgS and PbS nanoparticles

Junjie Zhu
, Suwen Liu
, O. Palchik
, Yuri Koltypin
, A. Gedanken

Department of Chemistry

Bar-Ilan University
Nanjing University

Research output: Contribution to journal › Article › peer-review

124 Scopus citations

Abstract

HgS and PbS nanoparticles of about 15 and 20 nm in size have been prepared by the sonochemical irradiation of an ethylenediamine solution of elemental S and mercury acetate or lead acetate under air. The nanoparticles are characterized using techniques such as transmission electron microscopy, X-ray diffraction, absorption spectroscopy, diffuse reflection spectroscopy, and energy-dispersive X-ray analysis. (C) 2000 Academic Press.

Original language	English
Pages (from-to)	342-348
Number of pages	7
Journal	Journal of Solid State Chemistry
Volume	153
Issue number	2
DOIs	https://doi.org/10.1006/jssc.2000.8780
State	Published - 2000

Bibliographical note

Funding Information:
Prof. A. Gedanken thanks the German Ministry of Science through the Deutche-Israeli Program (DIP) for its support and gratefully acknowledges receipt of a NEDO International Joint Research Grant. Dr. Zhu and Dr. Liu thank the Kort 100 Scholarship Foundation for supporting their postdoctoral fellowships. Drs. Zhu and Liu are also grateful for the support of the China Scholarship Council. The authors are grateful to Mr. G. Salitra for his help in the XPS measurements. The kind assistance of Dr. Siguang Chen and Dr. A. Zaban is gratefully acknowledged. We also thank Dr. Shifra Hochberg for editorial assistance.

Funding

Prof. A. Gedanken thanks the German Ministry of Science through the Deutche-Israeli Program (DIP) for its support and gratefully acknowledges receipt of a NEDO International Joint Research Grant. Dr. Zhu and Dr. Liu thank the Kort 100 Scholarship Foundation for supporting their postdoctoral fellowships. Drs. Zhu and Liu are also grateful for the support of the China Scholarship Council. The authors are grateful to Mr. G. Salitra for his help in the XPS measurements. The kind assistance of Dr. Siguang Chen and Dr. A. Zaban is gratefully acknowledged. We also thank Dr. Shifra Hochberg for editorial assistance.

Funders
German Ministry of Science
Kort 100 Scholarship Foundation
New Energy and Industrial Technology Development Organization
China Scholarship Council

Keywords

HgS
Nanoparticles
PbS
Sonochemistry

Access to Document

10.1006/jssc.2000.8780

Cite this

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title = "A novel sonochemical method for the preparation of nanophasic sulfides: Synthesis of HgS and PbS nanoparticles",

abstract = "HgS and PbS nanoparticles of about 15 and 20 nm in size have been prepared by the sonochemical irradiation of an ethylenediamine solution of elemental S and mercury acetate or lead acetate under air. The nanoparticles are characterized using techniques such as transmission electron microscopy, X-ray diffraction, absorption spectroscopy, diffuse reflection spectroscopy, and energy-dispersive X-ray analysis. (C) 2000 Academic Press.",

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note = "Funding Information: Prof. A. Gedanken thanks the German Ministry of Science through the Deutche-Israeli Program (DIP) for its support and gratefully acknowledges receipt of a NEDO International Joint Research Grant. Dr. Zhu and Dr. Liu thank the Kort 100 Scholarship Foundation for supporting their postdoctoral fellowships. Drs. Zhu and Liu are also grateful for the support of the China Scholarship Council. The authors are grateful to Mr. G. Salitra for his help in the XPS measurements. The kind assistance of Dr. Siguang Chen and Dr. A. Zaban is gratefully acknowledged. We also thank Dr. Shifra Hochberg for editorial assistance.",

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doi = "10.1006/jssc.2000.8780",

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AU - Liu, Suwen

AU - Palchik, O.

AU - Koltypin, Yuri

AU - Gedanken, A.

N1 - Funding Information: Prof. A. Gedanken thanks the German Ministry of Science through the Deutche-Israeli Program (DIP) for its support and gratefully acknowledges receipt of a NEDO International Joint Research Grant. Dr. Zhu and Dr. Liu thank the Kort 100 Scholarship Foundation for supporting their postdoctoral fellowships. Drs. Zhu and Liu are also grateful for the support of the China Scholarship Council. The authors are grateful to Mr. G. Salitra for his help in the XPS measurements. The kind assistance of Dr. Siguang Chen and Dr. A. Zaban is gratefully acknowledged. We also thank Dr. Shifra Hochberg for editorial assistance.

PY - 2000

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N2 - HgS and PbS nanoparticles of about 15 and 20 nm in size have been prepared by the sonochemical irradiation of an ethylenediamine solution of elemental S and mercury acetate or lead acetate under air. The nanoparticles are characterized using techniques such as transmission electron microscopy, X-ray diffraction, absorption spectroscopy, diffuse reflection spectroscopy, and energy-dispersive X-ray analysis. (C) 2000 Academic Press.

AB - HgS and PbS nanoparticles of about 15 and 20 nm in size have been prepared by the sonochemical irradiation of an ethylenediamine solution of elemental S and mercury acetate or lead acetate under air. The nanoparticles are characterized using techniques such as transmission electron microscopy, X-ray diffraction, absorption spectroscopy, diffuse reflection spectroscopy, and energy-dispersive X-ray analysis. (C) 2000 Academic Press.

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A novel sonochemical method for the preparation of nanophasic sulfides: Synthesis of HgS and PbS nanoparticles

Abstract

Bibliographical note

Funding

Keywords

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