A New Synthesis of Key Intermediates for the Preparation of 5,6‐DiHETE and Lipoxin A4

Agnès Gigou, Jean‐Paul ‐P Lellouche, Jean‐Pierre ‐P Beaucourt, Loïc Toupet, René Grée

Research output: Contribution to journalArticlepeer-review

29 Scopus citations

Abstract

The highly diastereoselective osmylation of a C  C bond in proximity to a complex fragment is the key step in the formation of 2 from the butadiene(tricarbonyl)iron complex 1. The diols 2 can be transformed readily into 3, key intermediates in the synthesis of 5,6‐DiHETE and lipoxin A4. R  SiPh2tBu; R′  Me; E  CO2Me. (Figure Presented.)

Original languageEnglish
Pages (from-to)755-757
Number of pages3
JournalAngewandte Chemie - International Edition
Volume28
Issue number6
DOIs
StatePublished - Jun 1989
Externally publishedYes

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